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Intramolecular schmidt reaction involving primary azidoalcohols under nonacidic conditions: Synthesis of indolizidine (-)-167B
, Erich Nyfeler, Guy Giuffredi T., Philippe Renaud
Published in
Volume: 131
Issue: 49
Pages: 17746 - 17747
(Chemical Equation Presented) A powerful intramolecular Schmidt reaction starting from primary azidoalcohols is reported. This approach involves a nonacidic activation of the alcohol via triflation. The synthetic potential offered by the mild reaction conditions is demonstrated by a highly selective synthesis of (-)-indolizidine 167B. {\textcopyright} 2009 American Chemical Society.
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